| 1. | The novel title compound was synthesized with benzaldehyde , isobutyraldehyde , phosphorus trichloride as raw materials . the total yield was 40 . 8 % . the structure was confirmed by 1h nmr , 31p nmr and elemental analysis
摘要以苯甲醛、异丁醛、三氯化磷为原料合成了新型的1 , 3 , 2 -氧磷杂环类化合物2 -苯羟甲基5 , 5 -二甲基4 -苯基2 -氧代1 , 3 , 2 -二氧磷杂环己烷，总收率为40 . 8 % ，并对其进行了nmr研究和结构表征。 |
